gc-ms Articles

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Analysis of PBDEs in Sediment Using GC-MS/MS

by Shimadzu Scientific Instruments Inc  (Nov. 19, 2012)

Polybrominated diphenyl ethers (PBDEs) are brominated flame retardants (BFRs) widely used in plastics. Due to their toxicity and persistence, their industrial production is to be eliminated under the Stockholm Convention. Contamination from PBDEs is widespread in the environment, including in sediments. In order to determine PBDEs in sediments, ...

GC-MS/MS Analysis of Pesticides in Drinking Water

by Shimadzu Scientific Instruments Inc  (Oct. 2, 2014)

According to Japan’s list of drinking water quality control substances, pesticides are included as supplemental items subject to analysis. Designed to complement the standards, the Ministry of Health, Labour and Welfare encourages water utilities to monitor pesticide levels and achieve specified targets. Among the 102 listed pesticides, 84 ...

Analysis of Opioids Using Isotope Dilution with GCMS-TQ8030 GC/MS/MS

by Shimadzu Scientific Instruments Inc  (Jul. 2, 2014)

Development of methods for analysis of drugs of abuse has become a high priority for both forensic toxicology and law enforcement. The large numbers of individual drugs and new "designer drugs" has made method development for these compounds a significant undertaking. Gas chromatography mass spectrometry (GCMS) has been used extensively for ...

GC/MS-SIM-An option for lower detection limits

by Curtis & Tompkins Laboratories  (Jul. 16, 2013)

Select Ion Monitoring mode (GC/MS-SIM) is a technique used to perform low level GC/MS measurements of organic compounds. GC/MS-SIM can reduce reporting limits 10-100 fold and can minimize the effects of matrix interferences.                                   ...

GC-MS Analysis of Polychlorinated Dibenzodioxins and Polychlorinated Dibenzofurans

by Sigma-Aldrich Co., LLC  (Jun. 5, 2012)

Polychlorinated dibenzodioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs) consist of 210 different compounds with varying degrees of toxicity, and the 17 congeners with chlorine substitution in the 2,3,7,8 positions are considered the most toxic. This chromatogram illustrates the separation of a 17 component 2,3,7,8-substituted PCDD and ...

airmoTWA: New Expert System for GC-FID/MS

by Chromatotec Group  (May 1, 2014)

Chromatotec has developed the first TRAP-GC-FID/MS designed for continuous monitoring of Volatile Organic Compounds (VOCs), inorganic molecules and permanent gases. In addition to the mass spectrometer (MS), this system encompasses the same trap, thermo desorption and separation technologies as airmoVOC analyzers (current mCERTS approved GCs ...

GC-MS Analysis Agricultural Pesticides on the SLB-5ms

by Sigma-Aldrich Co., LLC  (Dec. 31, 2006)

This application illustrates the analysis of 29 different agricultural pesticides of different classifications and functionalities, using the SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm  The analysis was done by GC-MS using selected ion monitoring (SIM) to allow detection of all compounds at 100 µg/L. The standard solution was made in ...

GC/MS analysis of a complex sample in DCM using hydrogen carrier gas

by Peak Scientific Instruments Ltd  (Jul. 2, 2014)

Labs worldwide have recently found that helium has been in short supply, leaving a number of labs without carrier gas. Added to this, helium prices have doubled over the past 10 years causing a number of labs to look into alternative carrier gases for GC, such as nitrogen and hydrogen. As well as lower price and unlimited availability, hydrogen ...

The extraction and quantification of limonene from citrus rinds using GC/MS

by PerkinElmer, Inc.  (Oct. 28, 2009)

D-Limonene, shown in Figure 1, is a common naturally occurring compound with a citrus scent. It is often used as an additive in food products and fragrances, and is classified by the U.S. Food and Drug Administration (FDA) as Generally Recognized as Safe (GRAS)1. It has also been approved by the U.S. Environmental Protection Agency (EPA) for usage ...

Solid Phase Microextraction of Organophosphate Insecticides and Analysis by Capillary GC/MS

by Sigma-Aldrich Co., LLC  (Dec. 31, 1999)

SPME was used to extract an aquatic sample for analysis of organophosphate insecticides by gas chromatography/mass spectrometry (GC/MS).  An SPME fiber coated with 8.5um of polyacryate yielded detection limits ranging from 0.10 to 0.56ug/L. SPME is a quick and highly sensitive sample preparation technique that eliminates the use of solvents. ...

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