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extraction chromatography Applications

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    DETERMINATION OF TOTAL PETROLEUM HYDROCARBONS (TPH) IN WATER BY FLUORIMETRIC METHOD

    Total petroleum hydrocarbons (TPH) is a term used to describe a large family of several hundred chemical compounds that originally come from crude oil; the main and most specific part of these compounds are non-polar and slightly polar hydrocarbons of the aliphatic, aromatic and alicyclic structure. These compounds are harmful to humans and animals if absorbed through the skin, ingested, and inhaled thus claiming the analytical control of THP content in water as a global issue. Quantification of TPH in water is typically done using rather expensive chromatography techniques. Lumex Instruments developed fluorimetric method for cost-effective petroleum hydrocarbons in water determination using FLUORAT-02 analyzer. The method is based on measuring the fluorescence intensity of oil products after their extraction from water phase by hexane.

    By Lumex Instruments Group based in Mission, BRITISH COLUMBIA (CANADA).

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    Analysis of VOC compounds in water by Purge & Trap or dynamic headspace

    Context & Challenges Volatile organic compounds (VOC) can be dissolved in water. Sometimes water is polluted and to study contamination of VOC in finished drinking water, VOC must be measured. Chromatotec® Solutions Chromatotec® has developed a specific system for the measurement of VOC in water: a Purge & Trap system, the airmoPURGE. The analyzer is coupled with a degasing system allowing the extraction of dissolved gases. The complete system is based on: - 502.2 method from US EPA – “Volatile organic compounds in water by purge and trap capillary column gas chromatography with photoionization and electrolytic conductivity detectors in series – Revision 2.1”. - 524.2 method from US EPA – “Measurement of purgeable organic compounds in water by capillary column gas chromatography/mass spectrometry – Revision 4.0”.

    By Chromatotec Group based in Val de Virvée, FRANCE.

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