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sample preparator Applications

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    Improved Reproducibility and Reduced Sample Preparation Time for the HPLC Analysis of Aflatoxins in Raw Peanut Paste

    The US FDA and international regulatory agencies have set contamination levels for aflatoxins in animal feedstuffs. Since Aspergillus may infect commodities pre-harvest, during storage or during processing, monitoring for aflatoxins in associated agricultural commodities at all stages of production is requisite. Field screening methods exist that are adequate to estimate contamination levels for aflatoxins. When additional confirmation or quantification is desired, chromatographic laboratory analysis is often necessary. Preparation of matrix samples prior to chromatographic analysis typically requires extraction and purification. Commonly, immunoaffinity columns (IAC), which employ a multi-step bind and elute mechanism to concentrate and purify aflatoxins, are used to purify matrix samples for subsequent analysis. Solid phase extraction (SPE), an alternate method which may use interference removal, can also be employed.

    By Merck KGaA, Darmstadt, Germany based in Darmstadt, GERMANY.

  • Sample preparation and pumping systems for wastewater treatment industry

    A wide range of sample acquisition and filtration systems are available to prepare even the most difficult of samples for reliable on-line analyser measurement. The correct choice is often critical to prevent analyser blockage and optimise performance. Cross Flow Filtration The PPM cross flow filter, is a simple in-line device used to protect an analyser from ingress of solids, for applications where sample quality is generally good but occasionally suspended solids may be present. The stainless steel filter removes solids above 50 micron size.

    By Pollution & Process Monitoring Ltd based in Sevenoaks, UNITED KINGDOM.

  • Improved Reproducibility and Reduced Sample Preparation Time for the HPLC Analysis of Aflatoxins in Raw Peanut Paste

    The US FDA and international regulatory agencies have set contamination levels for aflatoxins in animal feedstuffs. Since Aspergillus may infect commodities pre-harvest, during storage or during processing, monitoring for aflatoxins in associated agricultural commodities at all stages of production is requisite. Field screening methods exist that are adequate to estimate contamination levels for aflatoxins. When additional confirmation or quantification is desired, chromatographic laboratory analysis is often necessary. Preparation of matrix samples prior to chromatographic analysis typically requires extraction and purification. Commonly, immunoaffinity columns (IAC), which employ a multi-step bind and elute mechanism to concentrate and purify aflatoxins, are used to purify matrix samples for subsequent analysis. Solid phase extraction (SPE), an alternate method which may use interference removal, can also be employed.

    By MilliporeSigma based in Bellefonte, PENNSYLVANIA (USA).

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    Chromatography laboratory instrumentation for environmental analysis

    Determining pollutants in environmental and food matrices requires efficient sample preparation and analytics. BUCHI provide a wide selection of solutions for reliable, flexible and safe sample processing procedures in the laboratory work flow for environmental analysis.

    By BÜCHI Labortechnik AG based in Postfach, SWITZERLAND.

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    Chromatography laboratory instrumentation for pharmaceutical

    Drug discovery and development for pharmaceutical industries require safe, efficient and compliant sample preparations and analytics. BUCHI offers a variety of reliable solutions for regulated pharmaceutical laboratories.

    By BÜCHI Labortechnik AG based in Postfach, SWITZERLAND.

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    Analysis of Herbicides in Drinking Water

    Herbicides are used throughout the world to combat the growth of unwanted plant life. These polar compounds are hydrophilic, so they may find their way into drinking water sources. While gas chromatography has historically been the preferred technique for analysis of herbicides in water samples, the use of LC-MS/MS for this application is gaining acceptance. This is due to the power of MS/MS to provide detailed identification of multiple analytes, but also in part due to the variety of HPLC stationary phases that are available. In particular, several HPLC phases are available that provide great retention and peak shapes for polar analytes, such as herbicides, even under mostly aqueous mobile phase conditions. The combination of these factors may possibly eliminate need for time-consuming sample preparation.

    By Merck KGaA, Darmstadt, Germany based in Darmstadt, GERMANY.

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    Determination of Additives in Beverages using Ascentis Express Columns

    Beverages, such as sodas and energy drinks, can include a number of polar ingredients, which are easily soluble in the water matrix of the drinks. These ingredients include sweeteners (sugars and sugar substitutes), caffeine, vitamin supplements, amino acids, organic acids, and plant extracts. Because the analytes are already in solution, there is no need for extensive sample preparation. Dilution followed by direct injection into an HPLC is typically suitable. In this article we present two beverage applications using Ascentis Express HPLC columns. Ascentis Express columns offer faster HPLC on any system. One benefit is their ability to produce the resolution, efficiency, and speed on conventional HPLC systems that is associated with the use of sub-2 micron columns on a UHPLC system, without generating high backpressure. Column chemistries (RP-Amide and HILIC) were selected for this article based on their enhanced performance with polar compounds in comparison to C18.

    By Merck KGaA, Darmstadt, Germany based in Darmstadt, GERMANY.

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    Application package FLUXANA Silicon Carbide

    FLUXANA application packages include always the sample preparation method. All packages are running in our application laboratory. You are always free to send your samples for testing free of charge. If you combine our application packages with our sample preparation machines FLUXANA garanties the analytical performance of the package like a contract.

    By Fluxana GmbH Co. KG based in Bedburg-Hau, GERMANY.

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    Determination of anionic surfactants in water by fluorimetric method

    Anionic surfactants (A-SAS) represent, by volume, the most important group of surfactants used in cleaning products and the oldest and the largest volume anionic surfactant is soap. In concentrations 0.1 ~ 1.0 mg/L A-SAS become toxic for aquatic environment. Lumex Instruments provides sensitive and selective fluorimetric method for the measurement of mass concentration of anionic surfactants in water samples using the FLUORAT-02 analyzer. The method became the Interstate standard for anionic surfactant in water determination; the benefit of the method is that it doesn’t require expensive instrumentation and tedious sample preparation.

    By Lumex Instruments Group based in Mission, BRITISH COLUMBIA (CANADA).

  • Closed Vessel Digestion of Soil

    Aurora`s TRANSFORM series of microwave digestion systems, offers high-pressure and temperature systems in order to increase reaction rates and decrease digestion times for sample preparation for trace metal analysis in soil.

    By Aurora Biomed Inc. based in Vancouver, BRITISH COLUMBIA (CANADA).

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    EDXRF spectrometers for forensics industry

    Fingerprinting all kinds of materials analyzed in forensic analysis

    Forensic scientists generally require fast and non-destructive analysis of a very wide range of materials. Often these materials are presented in very small quantity, as evidence collected from a crime scene. Using ED-XRF allows to measure a wide range of elements and concentrations: C(6)-Fm(100), without any need of sample preparations. Samples can be measured in many different formats such as powder, solid, liquid or in thin films.

    By Xenemetrix Ltd. based in Migdal Haemek, ISRAEL.

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    EDXRF spectrometers for metal & ore

    Quality control of the various metal industry processes. Metal forms an essential material in modern manufacturing, metal products being used everywhere. Using ED-XRF allows to measure a wide range of elements and concentrations - C(6)-Fm(100) - without the need for sample preparations (heating or destroying the sample). Samples can be measured in the form of loose powders or pressed into pellets and ready for measurement within seconds.

    By Xenemetrix Ltd. based in Migdal Haemek, ISRAEL.

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    Application package FLUXANA RAW Professional

    This application package is a `ready to go` calibration kit for xrf instruments. Fusion technology is ideal for analysing oxidic materials like minerals or raw materials. It performs with the highest precision possible in xrf sample preparation. However, many laboratories cannot specify exactly what material they have to analyse. Therefore FLUXANA has created a wide range oxidic application program to allow complete analysis of the unknown material. The concentration ranges and elements of interest can be adapted to customer needs.

    By Fluxana GmbH Co. KG based in Bedburg-Hau, GERMANY.

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    RAPID ANALYSIS OF TOTAL MERCURY IN WASTE WATERS AND PROCESS WATERS WITH ELEVATED MERCURY CONTENT USING DIRECT PYROLYSIS TECHNIQUE

    A conventional standard method of total mercury determination in water using atomic absorption spectrometry (AAS) involves preliminary sample digestion that takes from 30 minutes to 8 hours depending on the digestion conditions. The use of a mercury analyzer RA-915M/RA-915+ with Zeeman background correction in combination with PYRO-915+ pyrolysis attachment provides direct determination of mercury in process and waste waters contaminated with mercury without digestion or any other sample preparation stages. The measuring method is based on thermal atomization of mercury from a sample using a PYRO-915+ attachment and its consequent determination by flameless AAS with Zeeman background correction using the RA-915M mercury analyzer. The total time needed for determination of mercury is not longer than 2 minutes. RA-915+/915M is compliant with US EPA 7473 and ASTM D7622 methods.

    By Lumex Instruments Group based in Mission, BRITISH COLUMBIA (CANADA).

  • Chromatography systems for food industries

    Food samples exhibit a challenge to analytical chemists to determine pesticide residues to meet food safety regulations in USA and EU. Therefore, more careful sample preparation is needed to successfully identify and quantify these compounds in food. Dikma offers SPE columns with different absorbent phases and QuEChERS method for sample pre-treament.

    By Dikma Technologies Inc. based in Lake Forest, CALIFORNIA (USA).

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    Application package FLUXANA Cement

    This application package is a `ready to go` calibration kit for xrf instruments. It can, for example, contain all parts to perform a complete cement calibration: - Calibration set cement prepared from CRM as glass beads - Calibration work performed by FLUXANA expert 2 days on site - 2x drift monitors for xrf instrument - 2x control samples for validation - Flux FLUXANA application packages include always the sample preparation method. All packages are running in our application laboratory. You are always free to send your samples for testing free of charge. If you combine our application packages with our sample preparation machines FLUXANA garanties the analytical performance of the package like a contract.

    By Fluxana GmbH Co. KG based in Bedburg-Hau, GERMANY.

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    Application package FLUXANA RAW

    This application package is a 'ready to go' calibration kit for xrf instruments. It can, for example, contain all parts to perform a complete raw material (oxidic materials) calibration with 14 elements for cement, glass, ceramic and raw materials industry: - Calibration set raw materials prepared from CRM as glass beads - Calibration work performed by FLUXANA expert 2 days on site - 2x drift monitors for xrf instrument - 7x control samples for validation - Flux FLUXANA application packages include always the sample preparation method. All packages are running in our application laboratory. You are always free to send your samples for testing free of charge. If you combine our application packages with our sample preparation machines FLUXANA garanties the analytical performance of the package like a contract.

    By Fluxana GmbH Co. KG based in Bedburg-Hau, GERMANY.

  • Filtration systems & solutions for biosciences and scientific industry

    The scientific community and in particular for that of the life science industries such as the medical, pharmaceutical  and healthcare, have a growing need for superior technologies and products in filtration, separation, purification, aeration and liquid transfer. The range of BioVyon materials and applications are continuously expanding, driven by new market requirements and available to both OEM and end user customers. Applications include separation or filtration for healthcare, medical and pharmaceutical products, shut off valves for catheters, diagnostic wick and sample preparation devices.

    By Porvair Filtration Group based in Fareham, UNITED KINGDOM.

  • Analysis of aqueous solutions

    IR-Spectroscopy is not limited to gases, solid materials and pure liquids but also facilitates the measurement of solutes in aqueous media. Though, due to the strong and temperature dependent absorption of water, the usage of conventional IR-transmission and ATR accessories is not very suitable for the analysis in water. The CONFOCHECK is a dedicated FT-IR system for the fast, easy and sensitive analysis of aqueous samples. Using this system, preparing, measuring and evaluating any aqueous sample takes typically about 1 minute.

    By Bruker Corporation based in Billerica, MASSACHUSETTS (USA).

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    Application package FLUXANA RAW- Glass

    This application package is a 'ready to go' calibration kit for xrf instruments. In the glass industry, raw materials have to be analysed together with the quality control samples from production. FLUXANA has created two basic programs Raw Materials (CS-0022) and Glass (CS-0016) for these two purposes, which can be individually adapted by the customer. The application package raw materials can, for example, contain: - Calibration set raw materials prepared from CRM as glass beads - Calibration work performed by FLUXANA expert 2 days on site - 2x drift monitors for xrf instrument - 6x control samples for validation - Flux FLUXANA application packages include always the sample preparation method. All packages are running in our application laboratory. You are always free to send your samples for testing free of charge. If you combine our application packages with our sample preparation machines FLUXANA garanties the analytical performance of the package like a contract.

    By Fluxana GmbH Co. KG based in Bedburg-Hau, GERMANY.

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