A large part of the chemical industry sectors, particularly industrial surface treatments, contributes to the contamination of water bodies with heavy metals. The environmental laws have been stringent regarding discharge of effluents containing these compounds. This study evaluated the removal of metals Ni(II) and Zn(II) by adsorption on activated bone char residue. To evaluate the adsorption capacity, experiments were performed using kinetics in a monocomponent system and adsorption isotherms in monocomponent and bicomponent systems. The models used to fit the isotherms were the Langmuir and Freundlich.