carbamate column Articles

  • 2.1 mm ID micro carbamates column ideal for LC-MS confirmation

    Post-column derivatization of carbamates with hydroxide and OPA is the method of choice for the detection of carbamates because of its high selectivity and high sensitivity (US EPA 531.1 & AOAC 985.23).  To confirm the finding of carbamates in the tested samples, there are various possibilitites: To confirm the finding of carbamates in the tested samples, there are various ...


    By Pickering Laboratories, Inc.

  • Quantitative application for OP/carbamate screen

    I. PURPOSE - The purpose of this document is to detail the standard operating procedure for the screening of cholinesterase inhibiting carbamate insecticides in fruits, vegetables, and feeds using the SDI Food Prep Kit and InQuest OP/Carbamate Screening Kit. NB - This is a screening technique designed to determine presence or absence of cholinesterase inhibiting ...


  • Pinnacle PCX Carbamate Testing at Nebraska Health

    Beta Site Evaluation of the EPA Carbamate in Drinking Water Method 531.1 with Pickering Laboratories Pinnacle PCX Integrated LC/Post-Column Derivatization Instrument. The Nebraska DHHS Public Health Environmental Laboratory conducts environmental testing for the state of Nebraska. It employs mandated U.S. Environmental Protection Agency (EPA) methods for the determination of regulated substances ...


    By Pickering Laboratories, Inc.

  • Expanded HPLC Method for N-Methyl Carbamates post-column analysis of pesticides in food and potable water samples

    Carbamate pesticides are widely used around the world to protect crops. In addition, they are used as biocides for industrial or other applications and in household products. Though carbamates are biodegradable compounds and bioaccumulation usually happens only to a low extend it is important to monitor produce to make sure enough time has elapsed between harvest and applying pesticides. Also, ...


    By Pickering Laboratories, Inc.

  • Post-Column LC analysis of 23 N-methyl carbamates an expanded method using water/acetonitrile or water/methanol gradients

    There are a number of carbamate pesticide compounds employed worldwide which are not included in the 10 compounds mandated by USEPA Method 531.1 and AOAC Protocol 29.A05. This Application Note describes methods for separating as many as 23 compounds, using a Pickering C8, 5µm silica, column with either Water/Acetonitrile or Water/Methanol gradients. Instruments, post-column derivatization ...


    By Pickering Laboratories, Inc.

  • Screening of fruits, vegetables, and feeds for carbamates - strategic diagnostics inc.’s, inquest op/carbamate screen

    I. PURPOSE - The purpose of this document is to detail the standard operating procedure for the screening of cholinesterase inhibiting carbamate insecticides in fruits, vegetables, and feeds using the SDI Food Prep Kit and InQuest OP/Carbamate Screening Kit. NB - This is a screening technique designed to determine presence or absence of cholinesterase inhibiting ...


  • A Simple and Ultra-Sensitive LC/MS/MS Method for Analysis of N-Methyl Carbamates in Water

    IntroductionN-methyl carbamate pesticides are widely used due to their broad range of activity. Water sources can be polluted bycarbamates through surface water runoff from areas such as agriculture fields, golf courses, and residential properties.Human and animal studies have suggested that long-term, low-level exposure to carbamates can cause adverse healtheffects, including ...


  • Fast LC-MS-MS Quantitation of N-Methyl Carbamate Pesticides in Food using Bond Elut® Plexa™ and Pursuit® XRs C18

    A fast quantitation method for the analysis of N-Methyl Carbamate pesticide residues in vegetables and grains has been developed with Bond Elut Plexa clean-up, Pursuit XRs C18 columns, and 320 LC-MSMS. High recoveries were obtained for most carbamates screened in all matrices tested at 1 ppb levels. Good linearity of the calibrationcurves was observed for all analytes, over the range from 1 ppb ...


  • Fast LC/MS/MS Quantitation of N-Methyl Carbamate Pesticides in Food Using Bond Elut™ Plexa™ and Pursuit™ XRs C18

    AbstractA fast quantitation method for the analysis of N-methylcarbamate pesticide residues in vegetables and grainshas been developed with Bond Elut Plexa clean-up, Pursuit XRs C18 columns, and 320-MS LC/MS/MS. Highrecoveries were obtained for most carbamates screened in all matrices tested at 1 ppb levels. Good linearity of thecalibration curves was observed for all analytes, over ...


  • o-Phthalaldehyde Reagent

    Introduction Primary amines form highly fluorescent adducts when reacted with o-Phthalaldehyde (OPA) and a mercaptan under basic conditions. At a pH>9 and ambient temperature, reaction is generally complete within 30 seconds. The products of this reaction, 1-alkyl-2-alkylthio-substituted isoindoles, exhibit optimal excitation at 330 nm and maximal emission at 465 nm. The reagents ...


    By Pickering Laboratories, Inc.

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