gas chromatograph mass spectrometer Articles

  • Ion Mobility Mass Spectrometry – Catch the Excitement!

    Interest in ion mobility mass spectrometry (IMS) technology is growing rapidly. The signs are everywhere. Since the year 2000, the number of abstracts submitted to ASMS mentioning ion mobility has grown more than 10-fold – from 30 to more than 350 in 2015. For most of that time, ion mobility has been available commercially in high-end research instruments or in homemade platforms. Waters ...


    By Waters Corporation

  • Mass balance analysis of triclosan, diethyltoluamide, crotamiton and carbamazepine in sewage treatment plants

    The behavior of antibacterial triclosan, insect-repellent diethyltoluamide (DEET), anticonvulsant carbamazepine, and antipruritic crotamiton was investigated at two sewage treatment plants (STPs) to clarify their complete mass balance. Twenty-four-hour flow-proportional composite samples were collected from the influent and effluent of primary and final sedimentation tanks, a biofiltration tank ...


    By IWA Publishing

  • Environics - Reducing calibration gas cost by up to 60%

    EPA's appendix 'M' 40 CFR 51 reduces calibration gas cost by 60%By: Terrence P. Dunn, President of EnvironicsOn May 30, 1995, the EPA published the final version of Method 205 for inclusion in Appendix M of 40 CFR Part 51 entitled, 'Verification of Gas Dilution Systems for Field Instrument Calibrations.' Continuous emissions monitoring systems (CEMS) require ...


    By Environics, Inc.

  • Gas cell selection for analysis of electronic gases

    APIMS and FTIR remain the preferred analytical tools for monitoring impurities in the electronic  specialty gases used by the semiconductor industry, although other tools such as CRDS are currently finding application in selected cases. FTIR spectroscopy offers the advantage of the simultaneous measurement of all gaseous species that exhibit dipole moment changes during vibrations at ...


    By CIC Photonics, Inc.

  • Development of a novel odor measurement system using gas chromatography

    This paper describes a novel odor measurement system for creating arrays of virtual chemical sensors with nonoverlapping responses using ultrahigh-speed gas chromatography with a surface acoustic wave sensor (GC/SAW). This GC/SAW system provides high-resolution twodimensional olfactory images for easy recognition of many complex odors. Separation and quantification of the individual chemicals ...

  • Fenton degradation of Cartap hydrochloride: identification of the main intermediates and the degradation pathway

    The advanced oxidation of Cartap hydrochloride (Cartap) promoted by the Fenton system in an aqueous medium was investigated. Based on total organic carbon, chemical oxygen demand and high-performance liquid chromatography, the oxidation of Cartap is quite efficient by the Fenton system. Its long chain is easily destroyed, but the reaction does not proceed to complete mineralization. Ion ...


    By IWA Publishing

  • Fenton degradation of Cartap hydrochloride: identification of the main intermediates and the degradation pathway

    The advanced oxidation of Cartap hydrochloride (Cartap) promoted by the Fenton system in an aqueous medium was investigated. Based on total organic carbon, chemical oxygen demand and high-performance liquid chromatography, the oxidation of Cartap is quite efficient by the Fenton system. Its long chain is easily destroyed, but the reaction does not proceed to complete mineralization. Ion ...


    By IWA Publishing

  • Semi-volatile organics in drinking water using EPA method 525.2 optimized for greater sensitivity

    The US EPA Drinking Water Manual contains the methods used to identify and quantify regulated and unregulated organic drinking water contaminants. Included in this manual is Method 525.2, a Gas Chromatographic/ Mass Spectrophotometric (GC/MS) technique for the determination of semi-volatile organic compounds. Method 525.2 can be used for the identification and quantification of a group of ...


    By PerkinElmer, Inc.

  • U.S. EPA volatile organics method 524.2 using PURGE and TRAP GC/MS

    Clean drinking water is of worldwide interest. Contaminants can compromise the quality of a water supply and cause short- and long-term health effects. Stringent water quality criteria help to ensure safe drinking water by requiring the detection and quantification of a wide variety of contaminants at extremely low levels. U.S. EPA Method 524.2 (1) provides the guidance necessary for identifying ...


    By PerkinElmer, Inc.

  • Instrumental methods and challenges in quantifying

    Abstract Increased interest in the fate, transport and toxicity of polybrominated diphenyl ethers (PBDEs) over the past few years has led to a variety of studies reporting different methods of analysis for these persistent organic pollutants. Because PBDEs encompass a range of vapor pressures, molecular weights and degrees of bromine substitution, various analytical methods can lead to ...


  • Texas Instruments - A Novel Separation Technique for the Analysis of Trace Levels of Atmospheric Contaminants in Inert Semiconductor Process Gases

    A NOVEL SEPARATION TECHNIQUE FOR THE ANALYSIS OF TRACELEVELS OF ATMOSPHERIC CONTAMINANTS IN INERTSEMICONDUCTOR PROCESS GASES J. Scott McWilliams, Alan Johnson, Charlene Long, Jeremiah D. Hogan*Texas Instruments, Inc.Dallas, TX 75265 Low ppb detection limits for contamination in cylinder gases have been achieved with gas chromatography using a modified gas ...


    By Environics, Inc.

  • Detection and measurement of GWGs in semiconductor fab facilities

    Problem Statement Various processes and tools in the modern wafer fab plant produce effluent streams that contain unacceptably high levels of perfluorocarbon GWGs (greenhouse warming gases). These effluent streams are abated by plasma incineration and wet scrubbers and other techniques. It is necessary to measure the destruction removal efficiency (DRE) of the various abatement methods ...


    By CIC Photonics, Inc.

  • Assessment of the PAHs contamination threat on groundwater: a case study of the Niger Delta region of Nigeria

    Contamination of the environment by polynuclear aromatic hydrocarbon (PAHs) is becoming a rising environmental concern. The interest this subject attracts has continually increased by the day because of the threat these compounds pose to human health. Water samples from several hand-dug wells in the Niger Delta region of Nigeria where extensive crude oil production activities take place were ...


    By Inderscience Publishers

  • Thermal Desorption-GC/MS Analysis of polycyclic aromatic hydrocarbons on fine particulates in air

    Polycyclic aromatic hydrocarbons (PAHs) are commonly found throughout the environment in soil, water and adsorbed to fine particulate matter in air. Of the 16 common PAHs, 7 have been classified as animal carcinogens by the International Agency for Research on Cancer (IARC). Resulting from this classification, PAHs are monitored and regulated in the environment. Analysis of PAHs in soil and water ...


    By PerkinElmer, Inc.

  • TVOC measurement for LEED/green building evaluation

    Total Volatile Organic Compounds (TVOC) may be evaluated when building designers/managers are pursuing the Leadership in Energy and Environmental Design Green Building Rating System for New Construction (LEED-NC) EQ Credit 3.2. The latest LEED-NC guidance document specifies that the maximum allowed concentration of TVOC measured in a building (post construction, pre-occupancy) is 500 µg/m3; the ...


  • Is Microflow LC a Reality or Perception?

    Microflow or nanoflow chromatography has been used mostly in the academic and fundamental research environment in the past for its various advantages over analytical liquid chromatography, but rarely in the industrial settings. This is most likely because many of us believe it is a pain-in-the-neck technique to perform! But is this a reality or just a ...


    By Waters Corporation

  • Air Monitoring for the Gulf Oil Spill

    Ambient air monitoring is a priority in the ongoing efforts to contain and manage the oil spill from the Deepwater Horizon in the Gulf of Mexico. The following provides information about the kinds of airborne contaminants that are currently being monitored in the Gulf, how they are collected and how they are analyzed. For a given project, a suitable sampling plan – developed by ...


  • Large Volume Splitless Injection Using an Unmodified Split/Splitless Inlet and GC-TOFMS for Pesticides and Brominated Flame Retardants

    Abstract Large volume splitless injection for gas chromatography typically requires a special injection port, for example, a programmable temperature vaporizer (PTV), but an alternative setup using concurrent solvent recondensation–large volume splitless injection (CSR-LVSI) and a split/splitless injection port has been reported. This technique was used here, both with and without ...


    By Restek Corporation

  • How Can TO-15 Help You Solve Your Next IAQ Problem?

    Untitled Document Have you ever been asked to investigate unpleasant odors in a home or at the workplace? Are occupants developing headaches or a feeling of nausea? ...


    By EMSL Analytical, Inc.

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