hplc control Articles

  • Determination of Additives and Preservatives in Beverages by Isocratic HPLC

    The Earth is 75% water, as are most life forms on Earth. People need to drink several quarts of water a day to live well, and most of us prefer to consume beverages other than water to satisfy our thirst. Soda (or Pop depending on your location) is the primary drink of the average American; and all Soda is manufactured (as opposed to coming out of the ground from a spring in Maine). As such, ...


    By Buck Scientific Inc

  • Analysis of Organic plating Bath Additives and Chemicals by Isocratic HPLC

    In today’s world, over 75% of all metal surfaces on manufactured metal “items” have some sort of plated finish on them. From highchromium steel car bumpers to zinc diecast toys to Silver-contact electronic components. While the primary composition of these plating baths are inorganic (the metals and salts that are used to make up the desired metal finish), almost all types of plating baths; from ...


    By Buck Scientific Inc

  • Analysis of atrazine and its degradation products in loamy soil by SPE and HPLC

    The degradation and leaching of atrazine and its degradation products (hydroxyatrazine, desethylatrazine, deisopropylatarzine and didealkylatrazine) were studied into loamy soil. An agriculture soil field (50 × 50 sq. feet with brinjal plants) was selected and atrazine spray was carried out once in a year. The irrigation of this plot was carried out once in a month. The sampling of soil was ...


    By Inderscience Publishers

  • The development of cation-exchange chromatography in free amino acids analysis

    Although it was not called a liquid chromatograph, the first such instrument was introduced in late 1959 by Beckman Instruments and was designated the M.S. Amino Acid Analyzer in honour of Moore and Stein. Inject valves had yet to be invented, the buffer switching valves were glass stopcocks and the column temperature was controlled by circulating water baths. Two positive displacement pumps ...


    By Pickering Laboratories, Inc.

  • o-Phthalaldehyde Reagent

    Introduction Primary amines form highly fluorescent adducts when reacted with o-Phthalaldehyde (OPA) and a mercaptan under basic conditions. At a pH>9 and ambient temperature, reaction is generally complete within 30 seconds. The products of this reaction, 1-alkyl-2-alkylthio-substituted isoindoles, exhibit optimal excitation at 330 nm and maximal emission at 465 nm. The reagents ...


    By Pickering Laboratories, Inc.

  • Solid-state fermentation for production of gibberellic acid using agricultural residues

    Solid-State Fermentation (SSF) was employed using agricultural residues, viz. pigeon pea pod (Cajanus cajan), corncobs (Zea mays), sorghum straw (Sorghum vulgare) and pea pod (Pisum sativum) for the production of gibberellic acid (GA3) using Fusarium proliferatum NCIM1105. Studies revealed that these agricultural residues have supported excellent growth of the fungi in modified medium and gave ...


    By Inderscience Publishers

  • A bridge with our customers - Prominence-i (i-Series) - Case Study

    Anthem Biosciences, which is ranked among the top 5 leading Contract Research Organisations (CROs) in India, is emerging as a global leader in the domain of Integrated Pharmaceuticals business. Anthem, which calls itself a Contract Research and Innovation Service Provider (CRISP), offers a whole gamut of services dedicated to enabling and sustaining global research efforts in the discovery of new ...

  • Degradation of azo dyes in water by Electro-Fenton process

    Abstract The degradation of the azo dyes azobenzene, p-methyl red and methyl orange in aqueous solution at room temperature has been studied by an advanced electrochemical oxidation process (AEOPs) under potential-controlled electrolysis conditions, using a Pt anode and a carbon felt cathode. The electrochemical production of Fenton's reagent (H 2O 2, Fe 2+) allows a controlled in situ generation ...


    By Springer

  • Developing equipment specific lockout/tagout procedures – Case Study

    Challenge: Antea®Group was contracted by one of the world’s largest chemical manufacturing organizations to provide equipment-specific lockout / tagout procedures at their largest Research and Develop facility in North America. The overall objective of the project was to evaluate the worker risks during maintenance and repair operations associated with laboratory ...


    By Antea Group - USA

  • Rapid raw material identification for formulation compounds using handheld Raman technology

    Ever since the European Medicines Agency (EMA) recommended that all pharmaceutical companies test every raw material that passes through their manufacturing facilities, this practice has attracted great interest in the nutraceuticals, food manufacturing, cosmetics, and agricultural industries, pushing them to strive for more rigorous and technology-oriented quality control standards. In recent ...


    By B&W Tek

  • Clean your test sieves to maintain accurate results

    A standard process in analytical laboratories is sieve analysis, the practice of accessing the particle size distribution of a granular material. The trouble is, sieves prove quite the challenge to clean thoroughly enough to get all the contaminants out of the mesh. Every last grain stuck in the sieve must be removed to gain accurate analysis. A solution has been found in the use ...


    By Camlab Limited

  • Calibration of a passive, in situ, integrative sampler for monitoring of microbial biotoxins in aquatic environments

    In this work, an integrative passive sampler based on a silicone membrane filled with a suspension of γ-Fe2O3 at pH 3.5 was developed. The novel device was calibrated for the measurement of microcystin concentrations in water. Laboratory calibration studies of the passive sampling devises under controlled conditions of temperature, water turbulence, and analyte concentration were ...


    By IWA Publishing

  • Materials Testing Laboratory Provides Cutting Edge Contamination Testing Solutions

    Many industries have extremely tight parameters for any contamination of parts that are used in their manufacturing process.  Testing for contamination and quality control is an integral part of these companies’ final products. At EMSL Analytical, the Materials Testing Laboratory has extensive experience in providing highly detailed analytical services to assist manufacturers in ...


    By EMSL Analytical, Inc.

  • Manufacturers face challenges with pharmaceutical impurities

    Pharmaceutical manufacturers may face various challenges when attempting to meet the United States Pharmacopeia (USP) requirements for residual solvents (volatile organic chemicals).Residual solvents in pharmaceuticals are trace level impurities of volatile organic compounds in final products or excipients. In general, residual solvents originate from manufacturing processes related to the ...


  • RaPID Assay PAH in soil application

    Intended Use For detection of Polynuclear Aromatic Hydrocarbons (PAHs) (as phenanthrene) in soil. For testing in other matrices, please contact our technical support department at 1-800-544-8881. Materials Required but Not Provided SDI Sample Extraction Kit (Part Number: A00160EA/A00160EB) Procedural Notes and Precautions ...


  • RaPID Assay carcinogenic PAHs in soil application

    Intended Use For detection of Carcinogenic PAHs (as benzo(a)pyrene) in soil. For testing in other matrices, please contact our technical support department at 1-800-544-8881. Materials Required but Not Provided SDI Sample Extraction Kit (Part Number: A00204EA/A00204EB) Procedural Notes and Precautions Prepare ...


  • Preparation of thiabendazole standards for use in applications of the benomyl/carbendazim rapid assay

    GENERAL COMMENTS: This procedure describes the preparation of thiabendazole (TBZ) standards used in applications of the Benomyl/Carbendazim RaPID Assay. Standard concentrations of 10, 50 and 250 ng/mL (ppb) TBZ and a control concentration of 100 ppb TBZ are prepared by making appropriate dilutions of a concentrated TBZ solution in the Benomyl/Carbendazim Sample Diluent. The standards and ...


  • USLC columns put the right tools in your LC method development toolbox

    Understanding Selectivity in Reversed Phase Separations – A Simplified Approach to HPLC and UHPLC Column Selection The most significant influence on chromatographic peak separation, or resolution, is column selectivity. Unfortunately, column selectivity is also the least understood and most underutilized parameter. To improve selectivity, method developers often concentrate on ...


    By Restek Corporation

  • Toxicity Identification Evaluation (TIE) as a Tool for Water Quality Management

    Whole effluent toxicity (WET) testing has evolved into a critical element of many National Pollutant Discharge Elimination System (NPDES) permits issued to both industrial and municipal dischargers. Over 6,500 dischargers to both fresh and salt waters are required to conduct toxicity tests to determine if their effluent might be potentially toxic to organisms in the receiving system. While ...


    By AECOM

  • LC/MS/MS analysis of metabolites of synthetic Cannabinoids JWH-018 and JWH-073 in Urine

    Abstract A liquid chromatographic method was developed to resolve a comprehensive set of metabolites of JWH-018 and JWH-073. In addition to the chromatographic analysis method, an extraction method was developed to recover a broad range of synthetic cannabinoid metabolites, including carboxylic acid metabolites that are not traditionally recovered using a high pH liquid/liquid extraction. ...


    By Restek Corporation

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