HPLC sample Articles
-
Carbonyl Sampling and Analysis by HPLC
Sampling of Carbonyls Using a Dual-Layer LpDNPH Glass Sampling Tube and HPLC Analysis with an Ascentis Express C18 Column The dual-layer LpDNPH ORBO-555 tube is an effective sampler for measuring airborne carbonyl concentration. The low background levels in the sampler allow for accurate measurements of low concentration samples or samples collected in situations where short sampling times are ...
-
News on Air 2013, Volume 1: Products for Sampling
For decades, Sigma-Aldrich has been a key supplier of innovative & high technology air monitoring products for various areas of gas/air sampling. Enclosed, you will find an overview on new and interesting devices to improve or simplify your air sampling. Supelco and Sigma-Aldrich offer a range of active and passive air sampling products, in addition to various analytical chemistry tools ...
-
Analysis of Tetrahydrocannabinol Vape Oils Using Pyroprobe by Thermal Extraction
Abstract This application note demonstrates a multi-step thermal extraction study on Tetrahydrocannabinol (THC) vape oils. Introduction E-cigarettes have gained popularity in recent years, in conjunction with the legalization of marijuana in many U.S. states. Authentic THC vape oils are not easily distinguishable from the counterfeits, which are poorly regulated and can cause severe lung ...
-
HPLC prep - which filter fits your chromatography sample best?
Sample filtration protects your HPLC column and preserves data quality. Read our tips on filter and solvent selection and the use of tools to save time in HPLC prep, improve lab efficiency, and better your analytical chemistry techniques. Filtering samples prior to high-performance liquid chromatography (HPLC) analysis can help avoid frit clogging while maintaining data quality. Adding a ...
By Cytiva
-
Reverse-phase HPLC method for the simultaneous analysis of triclosan and triclocarban in surface waters
A validated reverse-phase HPLC-DAD for the simultaneous determination of triclosan and triclocarban in surface water has been developed, because this method has not been used for determination of these disinfectant agents so far. An isocratic elution was achieved using a Develosil RP Aqueous AR-5 RP-30 column with a flow rate of 1.0 mL min−1. The mobile phase consisted of mixed methanol and water ...
-
Sampling of Carbonyls Using a Dual-Layer LpDNPH Glass Sampling Tube and HPLC Analysis
The dual-layer LpDNPH sorbent tube is an air sampling device designed for sampling carbonyls (e.g. formaldehyde) in ambient, indoor, and industrial atmospheres. Carbonyls are trapped on our high-purity silica gel adsorbent coated with 2,4-dinitrophenylhydrazine (2,4-DNPH) where they are converted to stable hydrazone derivatives. The derivatives are eluted from the tube in acetonitrile and ...
-
Clean your test sieves to maintain accurate results
A standard process in analytical laboratories is sieve analysis, the practice of accessing the particle size distribution of a granular material. The trouble is, sieves prove quite the challenge to clean thoroughly enough to get all the contaminants out of the mesh. Every last grain stuck in the sieve must be removed to gain accurate analysis. A solution has been found in the use of ultrasonic ...
-
Cannabis quality tests now much faster thanks to HPLC
A new method of measuring phytocannabinoids has been developed and HPLC has been found to hold the key to faster measurements times. Read on to learn more and to discover our nitrogen generators for HPLC – ELSD. Researchers from the University of British Columbia have created a new method of measuring phytocannabinoids which is more than twice as quick as traditional methods. ...
-
Predicting the Toxicity of Oil-Shale Industry Wastewaters by its Phenolic Composition
Abstract : The chemical composition and toxicity of five phenolic wastewaters samples collected from the Kohlta-Järve (Estonia) oil-shale industry region were analysed. The total phenolic contents (HPLC data) of these samples ranged from 0.7 mg/l to 195 mg/l. A total of 11 phenol (up to 84 mg/l) and p-cresol (up to 74 mg/l). Artificial phenolic mixtures were also composed, to mimic the ...
-
Development of a Cleaning Validation Method for MICRO® A07 Citric Acid Cleaner Using HPLC-CAD
Abstract A high performance liquid chromatography (HPLC) method with a Corona Charged Aerosol detector for the cleaning validation of MICRO* A07 Citric Acid Cleaner residue has been developed. The pooled average repeatability of 3 replicates at 6 concentration levels expressed as RSD was 1.3 % while the pooled average intermediate precision (intra-day repeatability in 3 days) of 3 replicates at 6 ...
-
Introducing Sterlitech’s Expanded Range of Syringe Filters
Sterlitech Syringe Filters play important roles in the purification processes inside laboratories and out in remote operations—applying to sample preparation for HPLC, pharmaceutical dissolution testing, and environmental monitoring, to name a few. Industries and applications that use syringe filters continue to transform and expand, with the market expected to grow at 3.3%(1) for the ...
-
Hollow-fiber-supported liquid-phase microextraction using an ionic liquid as the extractant for the pre-concentration of bisphenol A, 17-β-estradiol, estrone and diethylstilbestrol from water samples with HPLC detection
A new method for the determination of four endocrine disrupting compounds (EDCs) (bisphenol A, 17-β-estradiol, estrone and diethylstilbestrol) in water samples has been developed using polypropylene hollow-fiber-supported ionic liquid (IL, 1-Octyl-3-methylimidazolium hexafluorophosphate, [C8MIM][PF6]) microextraction [HF-liquid-phase microextraction (LPME)] combined with high-performance ...
-
Photodegradation of microcystin-LR catalyzed by metal phthalocyanines immobilized on TiO2-SiO2 under visible-light irradiation
Microcystins (MCs) are a group of monocyclic heptapeptide toxins produced by species of cyanobacteria. Since MCs exhibit acute and chronic effects on humans and wildlife by damaging the liver, they are of increasing concern worldwide. In this study, we investigated the ability of the phthalocyanine compound (ZnPc-TiO2-SiO2) to degrade microcystin-LR (MC-LR) in the presence of visible light. ...
-
Extraction of trace tilmicosin in real water samples using ionic liquid-based aqueous two-phase systems
The effective method of ionic liquid-based aqueous two-phase extraction, which involves ionic liquid (IL) (1-butyl-3-methyllimidazolium chloride, [C4mim]Cl) and inorganic salt (K2HPO4) coupled with high-performance liquid chromatography (HPLC), has been used to extract trace tilmicosin in real water samples which were passed through a 0.45 μm filter. The effects of the different types of ...
-
Photochemical degradation of 4-chlorophenol in the aqueous phase using peroxyacetic acid (PAA)
The photochemical degradation of 4-chlorophenol (4-CP) using ultraviolet irradiation (UV) of 6, 12 and 18 W with peroxyacetic acid (PAA) was studied in a batch reactor. The objective of this work was to investigate degradation and mineralization of 4-CP by PAA. The degradation efficiency increased with increasing UV input. The degradation process was also pH and initial PAA concentration ...
-
The Toxicity of Cyanobacterial Blooms as Determined by Microbiotests and Mouse Assays
Abstract : Cyanobactrial blooms are common throughout the world in eutrophic water bodies. Cyanobacterial hepato- and neurotoxins represent a health threat for humans as well as for animals in drinking water supplies. Mouse bioassays have been used extensively to detect cyanobacterial blooms toxicity but the use of warm-blooded vertebrates is limited to specialised laboratories and poses ethical ...
-
Solid-phase extraction of room-temperature imidazolium ionic liquids
Abstract Owing to their favorable properties, ionic liquids have recently gained recognition as possibly environmentally benign solvents. Now among the most promising industrial chemicals, they have already been labeled 'green' but this appellation seems due entirely to their very low vapor pressure. This growing interest in the various applications of ionic liquids will soon result in ...
-
Find out the principles of ELSD and the gas delivery solutions for ELSD from a nitrogen gas generator
ELSD is one of the most common detectors used with HPLC and is preferred to other detection methods for analyses such as carbohydrate, natural sugars and polymer analysis as well as being used for a wide range of other applications. As a mass-detector, ELSD has advantages over some other methods of detection such as UV detection that require analytes to contain chromophores and it is unaffected ...
-
Find out the principles of ELSD and the gas delivery solutions for ELSD from a nitrogen gas generator
ELSD is one of the most common detectors used with HPLC and is preferred to other detection methods for analyses such as carbohydrate, natural sugars and polymer analysis as well as being used for a wide range of other applications. As a mass-detector, ELSD has advantages over some other methods of detection such as UV detection that require analytes to contain chromophores and it is unaffected ...
-
Oxidative degradation of signature compounds and TOC reduction using advanced oxidation processes
ESCO International; a company specialising in Advanced Oxidation Processes, Ozone and UV systems and with the primary objective of resolving water pollution issues on a global scale, worked on a semi-pilot scale project with an internationally well-known company in the chemical & polymers production industry, based in US. Organic compounds of concern include BI, MI, BPA, HEG and NPI ...
Need help finding the right suppliers? Try XPRT Sourcing. Let the XPRTs do the work for you