oil sampling Articles

  • Recent Federal Developments

    TSCA/FIFRA EPA Extends Comment Period For Draft Guidance For Pesticide Registrants On Notifications, Non-notifications, And Minor Formulation Amendments: On October 5, 2017, the U.S. Environmental Protection Agency (EPA) issued a notice of extension of the comment period for the draft guidance  ...


    By Bergeson & Campbell, P.C.

  • Oil Sampling Best Practices

    Obtaining a representative oil sample from a closed loop lubrication system is essential to any good oil analysis program. As oil analysis programs become more standardized for routine monitoring, especially within equipment warranty support programs, equipment makers provide more sampling points on new equipment. These ...


    By Spectro Scientific

  • Train derailment prompts contaminated land investigation

    On March 30th 2015 a long freight train, transporting a variety of goods including lumber and chemicals, wound its way through the state of Mississippi. At around 5pm, part of the train failed to negotiate a curved portion of the track in a rural area near Minter City, resulting in the derailment of nine railcars, one of which leaked chemicals onto agricultural farmland and woodlands. Emergency ...


    By Gasmet Technologies Oy

  • Oil Sampling Best Practices (Part 2)

    Understanding Dynamic Particle Equilibrium in Closed Loop Systems Dynamic Equilibrium Condition (DEC) is defined as a steady state condition where the normal wear rate in a machine results in no net gain or loss of particles. ...


    By Spectro Scientific

  • Mineral oil contamination in dry food samples

    SpeedExtractor E-916: Optimization of pressurized solvent extraction (PSE) for the rapid and efficient determination of MOSH and MOAH in dry food samples Many food samples are contaminated with mineral oil coming from different sources. One possible source of contamination is the migration from cardboard packaging made of recycled fibers. Other sources of contamination with mineral oils ...


    By BÜCHI Labortechnik AG

  • GC Analysis of Crude Oil Samples in Compliance with ASTM D5307

    In the ASTM D5307 test method, crude oil containing components with boiling points to temperatures in excess of 538C (C44 or equivalent) are analyzed by a simulated distillation GC system by the internal standard method. A detailed boiling point distribution graph is created for the fraction with boiling points lower than 538C. The fraction with boiling points above 538C is calculated as ...

  • World Oil: Holistic optimization approach improves coring efficiency, sample quality

    To acquire a high-quality core in as few runs as possible, and reduce operational costs, a provider must maximize ROP while ensuring efficient, safe surface handling of the rock sample and coring assembly. To satisfy these requirements, HT30 Max, a full-gauge core barrel system with jam mitigation technology, has been introduced. To improve initial production and ultimate recovery, we must first ...


    By Baker Hughes, a GE company

  • Oil Recovery

    Industrial Wastewater Treatment Success Stories Oil Water Emulsion Wastewater Treatment Industry Oil Recovery - Improved Efficiencies A refinery was having several upsets in their ...


    By Integrated Engineers Inc.

  • Sample Preparation for Refuse Derived Fuels

    Plastic, wood and shredded waste, are in times of rising crude oil prices very interesting additions to the classic fuels. Especially in the cement industry, the energy rich fractions from conditioning processes are readily burned along. Important here is the analytical evaluation of the materials. Refuse derived fuels: Plastic, wood and shredded waste: Here are some examples of more or less well ...


    By Fritsch Milling and Sizing

  • Characterisation of water–oil drainage process through a reservoir rock sample by digital core analysis

    Oil–water relative permeability and capillary pressure of a water–wet digital core are computed using the finite–volume/volume of fluid method and mimicking traditional laboratory steady–state experiments carried out on a water saturated sample. Commercial software is used for immiscible multiphase fluid flow simulations, carried out on a low–cost multicore workstation, and the pore–scale data ...


    By Inderscience Publishers

  • New ASTM Test Method Offers Quick and Easy Oil and Grease Measurement for Water and Soil Samples

    Onsite Field Measurement of Oil and Grease A quick and easy field analysis method for determining oil and grease concentration levels is important for both offshore oil platforms and soil remediation sites.. Prior to the Montreal Protocol, infrared (IR) analysis using Freon as an extraction solvent was a widely used field and laboratory method. In 1999, the U.S. EPA promulgated Method 1664A ...


    By Spectro Scientific

  • Groundwater: Low-flow Purging and Sampling

    Significant timesavings, improved sample process integrity, quality assurance and minimal quantities of potentially contaminated purge water to manage - are attractive as the focus on groundwater quality sharpens and economics demand best cost-benefit based methods Water has become a vitally important resource.  Maintaining its quality and quantity and avoiding pollution are set to be ...

  • Measurement of naphthenic acids in the receiving waters around an offshore oil platform by passive sampling

    Polar organic chemical integrative samplers (POCIS) were deployed in the vicinity of an offshore oil installation and analysed for naphthenic acids (NA). POCIS accumulated a range of mono to tetracyclic NA, with different degrees of alkylation, with monocyclic acids being the most abundant. POCIS or similar polar samplers may currently be the only way to measure exposure to NA from offshore ...


    By John Wiley & Sons, Ltd.

  • Oil in Power Plant Wastewater

    The water is from the operations of a steam power plant located in the Bahamas. The water samples were taken from the Unit 31 (lower oil content) and Tank #3 (a higher oil content). The samples were tested and it was found through the jartesting procedures that the Floccin K was the best choice for floc size and water clarity. The Unit 31 was dosed at 0.5 gram in 1,000 ml and the Tank # 3 water ...


    By Integrated Engineers Inc.

  • Oil & Grease applications notes

    EPA Method 1664A & 1664Bwas developed to determine the precise amount of n-Hexane Extractable Material (HEM) and Silica Gel Treated n-Hexane Extractable Material (SGT-HEM) that exist within a water sample. The HEM or SGT-HEM that is extracted contains a mix of various hydrocarbons usually residing within the semi-volatile range with a boiling point greater ...


    By Horizon Technology, Inc.

  • Guide to Measuring Particles in Oil

    Particle counting is a critical aspect of any machine conditioning program and there are many tools out there available to monitor and track the quantity and severity of the contamination, be it due to external contamination or machine wear. The ...


    By Spectro Scientific

  • The analysis of polycyclic aromatic hydrocarbons in marine samples

    Polycyclic aromatic hydrocarbons (PAH) have been determined in marine samples for many years, but have only rarely been included in either national or international monitoring programmes. PAH can arise in the environment from natural sources, oil and petroleum products and combustion processes. Although oil spills influence PAH concentrations in local areas, the major sources of PAH are ...


    By Inderscience Publishers

  • On-site Oil Analysis to extend oil drain intervals

    Fleets demonstrate ROI on do it yourself oil analysis “If the oil is good, why would you change it?” Gary Lentsch, CAFM, fleet manager for Eugene Water & Electric Board (EWEB), asked ...


    By Spectro Scientific

  • Oil and grease in waste water

    Determination of oil and grease in waste water according to Standard Methods AWWA 5520 This Application Note describes the extraction and determination of oil and grease from waste water samples following Standard Methods 5520 part D (Soxhlet Extraction Method). “Oil and grease” is defined as any material recovered as a substance soluble in the solvent. Therefore, compounds ...


    By BÜCHI Labortechnik AG

  • Aldicarb in mint oil

    I. Preparation of Standards 1. Prepare a 10 mg/mL stock solution of aldicarb (Riedel de Haen) in methanol e.g. 100 mg aldicarb qs to 10 mL. Prepare a 20 ppm stock solution by diluting the 10 mg/mL stock solution 1:500 (20 mL of 10 mg/mL aldicarb qs 10 mL with methanol). 2. Label four 10 mL volumetrics: 0 standard, standard 1, standard 2, standard 3. 3. Add the appropriate volume of ...


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