sample preparation kit Articles

  • Sample extraction kit user’s guide

    Intended Use This extraction kit is for use with the appropriate immunoassay test kit. Each Sample Extraction kit contains the materials necessary to process twelve (12) soil or wipe samples. Test Principles The reagents contained in the Sample Extraction kit have been optimized for fast, efficient removal of compounds from soil or surfaces and convenient ...


  • Preparation of <25x or >100x dilutions with the rapid prep universal range extension kit

    GENERAL COMMENTS: This procedure describes how to prepare dilutions of less than 25x or greater than 100x using the appropriate RaPID AssaysÒ Sample Diluent and components of the RaPID PrepÔ Universal Range Extension Kit. Preparing dilutions of 25x to 100x are already described in the package insert of the Universal Range Extension Kit. Serial dilutions using components of the ...


  • When Consumables Kits are Greater Than the Sum of their Parts

    ProteinWorks and GlycoWorks kits address more than sample prep challenges One of the most challenging parts of an LC-MS workflow happens before analytical chemists even turn to their instrument: Sample preparation. Get it right, and the analytical run performs as expected. Get it wrong, and the assay has any number of problems, from poor sensitivity to poor reproducibility. The ...


    By Waters Corporation

  • Detection of chlorpyrifos in air using low volume polyurethane foam (PUF) sampling with immunoassay

    MATRIX: Air samples ANALYTE: Chlorpyrifos RANGE OF DETECTION: 0.088 to 1.200 mg/m3 MATERIALS: Chlorpyrifos RaPID AssayÒ Kit and Sample Diluent. Reagents: methanol (pesticide grade). Equipment: 40 mL glass vials with Teflon lined caps, 13 x 100 mm glass test tubes, 5 mL and 20 mL serological pipets, micropipet ...


  • Analysis of Trace Elements in Water by EPA Method 200.8 using ICP Mass Spectrometry

    This application note describes the methodology and use of the Shimadzu ICPMS-2030 ICP mass spectrometer for the analysis of trace elements in drinking and fresh waters following the EPA 200.8 method. This method is also used for analysis of wastewater. In-line addition of internal standards to calibration and unknown samples was accomplished using the Shimadzu Internal Standard Addition ...

  • Detection of PAH IN WATER using the ensys test system

    MATRIX: Water ANALYTES: PAH LIMIT OF DETECTION: 15 ppb MATERIALS: Ensys PAH Risc Soil Test Kit. Methanol (ACS Reagent Grade). Deionized water. Equipment: Ensys Field Accessory System. SAMPLE PREPARATION/ANALYSIS: Follow procedures are outlined in the Ensys PAH Risc Test Kit User’s ...


  • Detection of polychlorinated biphenyls (PCBs) in concrete using the dtech test system

    MATRIX: Concrete ANALYTES: Polychlorinated biphenyls (PCBs) RANGE OF DETECTION: DTECHTOR: 500 ppb to 25 ppm (as aroclor 1254). Color Card: 1 ppm to 25 ppm (as aroclor 1254) MATERIALS: DTECH PCB Test Kit. DTECH PCB Sample Extraction Kit. Reagents: table salt (sodium chloride) or salt packets used by restaurants ...


  • Aldicarb in mint oil

    I. Preparation of Standards 1. Prepare a 10 mg/mL stock solution of aldicarb (Riedel de Haen) in methanol e.g. 100 mg aldicarb qs to 10 mL. Prepare a 20 ppm stock solution by diluting the 10 mg/mL stock solution 1:500 (20 mL of 10 mg/mL aldicarb qs 10 mL with methanol). 2. Label four 10 mL volumetrics: 0 standard, standard 1, standard 2, standard 3. 3. Add the appropriate volume of ...


  • Detection of carbendazim in grapes matrix grapes

    ANALYTE: Carbendazim, a metabolite of benomyl RANGE OF DETECTION: 25 to 500 ppb MATERIALS: Benomyl/Carbendazim RaPID AssayÒ kit and Sample Diluent Food Prep Kit Reagents: acetone (pesticide grade) Equipment: homogenizer or blender with acetone resistant container cup, 50 mL polypropylene conical tubes, 13 x 100 mm glass test tubes, ...


  • Detection of captan in grapes

    MATRIX: Grapes ANALYTE: Captan RANGE OF DETECTION: 8 to 300 ppm MATERIALS: Captan RaPID AssayÒ kit and Sample Diluent Food Prep Kit Reagents: acetone (pesticide grade) Equipment: homogenizer or blender with acetone resistant container cup, 50 mL polypropylene conical tubes, 13 x 100 mm glass test tubes, ...


  • Analysis of PCB in water using the envirogard test system

    MATRIX: Water ANALYTE: PCB LIMIT OF DETECTION: Aroclor 1248: 1 ppm Aroclor 1260: 2 ppm Aroclor 1242: 2 ppm Aroclor 1254: 1.1 ppm BACKGROUND: This application describes a field screening method for determining PCB concentrations in water. A chemical reaction is induced that causes a color change ...


  • Detection of atrazine in fertilizers

    The Atrazine RaPID Assay, kit has been successfully applied to the determination of atrazine in fertilizer samples using the ollowing guidelines: 1. Weigh fertilizer into diluent. a) For each gram of fertilizer, use 10 mL of diluent. It is recommended that at least 1 g or up to 50 g of fertilizer be used to obtain a representative sample. b) As diluent use either a 50%(v/v) methanol: 50%(v/v) ...


  • RaPID Assay Cyclodienes in soil application

    Intended Use For detection of cyclodiene insecticides (as dieldrin) in soil. For testing in other matrices, please contact our technical support department at 1-800-544-8881. Materials Required but Not Provided SDI Sample Extraction Kit (Part Number: A00256EA) Procedural Notes and Precautions Prepare soil ...


  • Detection of carbendazim in soil

    MATRIX: Soil ANALYTE: Carbendazim, a metabolite of benomyl RANGE OF DETECTION: 37.5 to 750 ppb MATERIALS: Benomyl/Carbendazim RaPID Assay kit and Sample Diluent Reagents: methanol (pesticide grade), sodium hydroxide (ACS grade), distilled or deionized water. Equipment: reciprocating shaker, plastic bottles ...


  • Detection of carbaryl in soil

    MATRIX: Soil ANALYTE: Carbaryl RANGE OF DETECTION: 40 to 500 ppb MATERIALS: SDI Carbaryl RaPID AssayÒ kit and Sample Diluent. SDI RaPID PrepÔ Soil Collection Kit (optional). SDI RaPID PrepÔ Extraction Kit: Type II (extraction solution, optional) Reagents: Methanol (pesticide grade), distilled or ...


  • Detection of polychlorinated biphenyls (PCBS) in concrete

    MATRIX: Concrete ANALYTES: Polychlorinated biphenyls (PCBs) RANGE OF DETECTION: 500 ppb to 10 ppm MATERIALS: SDI PCB RaPID Assay® Kit. SDI RaPID Prep® PCB Sample Extraction Kit. SDI RaPID Prep Soil Collection Kit. Reagents: table salt (sodium chloride) or salt packets used by restaurants (e.g. Dixie ...


  • Case study - Canada crude oil sites

    The Canadian Council of Ministers of the Environment requires laboratories to use the CCME’s Petroleum Hydrocarbon (PHC) Method, where GC-FID instrumentation is used to report VPH and EPH hydrocarbon fractions. Sitelab’s popular Extended Diesel Range Organics (EDRO) test typically detects hydrocarbons in the C10 to C36 carbon range, but the UVF will pick up heavier compounds up to ...


    By Sitelab Corporation

  • Detection of pentachlorophenol in soil

    MATRIX: Soil ANALYTES: Pentachlorophenol (PCP) RANGE OF DETECTION: 100 ppb to 10 ppm MATERIALS: Pentachlorophenol RaPID AssayÒ kit and Sample Diluent Reagents: methanol (reagent grade), sodium hydroxide (ACS grade), distilled or deionized water. Equipment: reciprocating shaker, plastic bottles (polypropylene or ...


  • Dewatering of moist sediments and soils for application to RaPID Prep AND RaPID assays procedures

    BACKGROUND INFORMATION: High moisture content (>30% by weight) can significantly lower concentrations of analytes detected in the RaPID Prep soil methods. In these methods, water associated with a sample will increase the volume of the extraction solution (liquid phase) and decrease the amount of soil (solid phase) in a weighed sample. In some cases, water may also decrease the ...


  • Detection of atrazine in raw sugarcane juice

    MATRIX: Raw juice from sugarcane ANALYTE: Atrazine RANGE OF DETECTION: 50 ppb to 2.5 ppm MATERIALS: Atrazine RaPID Assay kit and Sample Diluent Equipment: micropipets, 100 and 500 μL; 13 x 100 mm glass test tubes, test tube rack. SAMPLE PREPARATION: As part of the sugar ...


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