sample preparation system Articles

  • Leader in sample preparation systems benefits from Axetris MFCs’ high dynamic range - Case Study

    Split ratio flexibility of GC injector increased 30-fold A leading manufacturer of analytical sample preparation systems in gas chromatography (GC) switched to Axetris MFCs - and in doing so, simplified their product range, while offering their customers at least 30 times more flexibility in split ratio. The market-leading dynamic range of Axetris mass flow controllers (MFCs)—with ...


    By Axetris Ag

  • PPCPs: Preparing for an uncertain regulatory future

    A recent study published in Environmental Pollution* identified 56 active pharmaceutical ingredients (APIs) in effluent samples from 50 large wastewater treatment plants across the U.S. Among the products found in samples were commonly prescribed anti-psychotic and antihypertensive drugs. As more studies continue to fuel public concerns over risks to public health and the environment, wastewater ...

  • Method Scaling in Preparative HPLC: Analytical Method & Preparative Method

    VOC:  “I tried to scale up my analytical HPLC method to prep and it didn’t work.” Andy:  This is one of the most common things we hear from chemists wanting to do preparative chromatography. We also hear the following question pretty often too: VOC:  “I have a good analytical HPLC method, how do I scale it to ...


    By Waters Corporation

  • Preparing for EPA’s mandatory reporting of greenhouse gases rule

    Recent action by the US EPA to finalize the Mandatory Reporting of Greenhouse Gases (GHG) Rule means that environmental managers must now seriously examine whether they are fully prepared to address the imminent requirements. This article provides some assistance by summarizing key points regarding the final versus proposed rule, providing clarification on key questions that have arisen since the ...


    By Trinity Consultants

  • Sample extraction kit user’s guide

    Intended Use This extraction kit is for use with the appropriate immunoassay test kit. Each Sample Extraction kit contains the materials necessary to process twelve (12) soil or wipe samples. Test Principles The reagents contained in the Sample Extraction kit have been optimized for fast, efficient removal of compounds from soil or surfaces and convenient ...


  • Preparation of Large-Size Cohesive Specimens for Calibration Chamber Testing

    This paper describes the design of an automated slurry consolidometer and calibration chamber system used to prepare largesize cohesive soil specimens for testing in-situ devices, model foundations, and ground anchors. A two-stage technique for the preparattion of homogeneous cohesive specimens subjected to a known stress history is described. Briefly summarized are the data acquisition/control ...


    By ASTM International

  • The 10 Key Factors in Selecting a Stack Sampling Firm

    Summary: This document is a summary of the key factors that you should take into consideration when hiring a stack testing firm.This has been prepared in conjunction with the ASTM criteria for standard practice of testing companies.The ASTM criteria has been supplemented, based on 125 years of direct testing experience, which is the combined years of experience of the individuals that contributed ...

  • USEPA Method 8260C using the Tekmar Atomx Automated VOC Sample Prep System and a Thermo Focus/DSQ™ II GCMS

    The United States Environmental Protection Agency (USEPA) developed Method 8260 to determine the concentration of Volatile Organic Compounds (VOCs) in water and soil matrices. USEPA Methods 5030 and 50351 are used to prepare water, soil and waste samples for analysis by USEPA Method 8260. USEPA Method 8260 was recently updated from 8260B to 8260C2. In this study water and soil sample analysis ...


    By Teledyne Tekmar

  • An In-Home Video Study and Questionnaire Survey of Food Preparation, Kitchen Sanitation, and Hand Washing Practices

    Foodborne illnesses pose a problem to all individuals but are especially significant for infants, the elderly, and individuals with compromised immune systems. Personal hygiene is recognized as the number-one way people can lower their risk. The majority of meals in the U.S. are eaten at home. Little is known, however, about the actual application of personal hygiene and sanitation behaviors in ...

  • Sampling and On-Site Analytical Methods for Volatiles in Soil and Groundwater - Field Guidance Manual

    Abstract: Volatile organic compounds (VOCs) are among the most frequently identified contaminants in soil and groundwater samples obtained during the investigation of suspected hazardous waste sites. Because some VOCs and their degradation products are potentially mutagenic, carcinogenic, or teratogenic, their concentrations in these two matrices are key factors in the risk assessment process. ...


    By QED Environmental Systems

  • Sample Handling Strategies for Accurate Lead-In-Soil Measurements in the Field and Laboratory

    ABSTRACT The inhomogenous lead-in-soil matrix can present serious obstacles to accurate sample collection and handling. In typical lead-in-soil measurement, particle size related errors in sampling and sample handling often exceed all other sources of error. The magnitude of error can vary widely depending on the particulate nature of the lead contaminant and the effectiveness of control ...

  • Low-Flow (Minimal Drawdown) Ground-Water Sampling Procedures

    Untitled Document Background The Regional Superfund Ground Water Forum is a group of ground-water ...


    By Solinst Canada Ltd.

  • News on Food 2013, Volume 2: Simplify Sample Prep, and Increase Speed and Sensitivity

    Analytical testing is used 1) to determine nutritional value and quality and 2) to ensure food safety and security. We have developed and continue to develop, specialized products that allow food analysts to simplify sample prep, and increase speed and sensitivity for many food and beverage applications. In this second issue of “News On Food”, we will focus on our continuously ...


    By MilliporeSigma

  • Detection of chlorpyrifos in air using low volume polyurethane foam (PUF) sampling with immunoassay

    MATRIX: Air samples ANALYTE: Chlorpyrifos RANGE OF DETECTION: 0.088 to 1.200 mg/m3 MATERIALS: Chlorpyrifos RaPID AssayÒ Kit and Sample Diluent. Reagents: methanol (pesticide grade). Equipment: 40 mL glass vials with Teflon lined caps, 13 x 100 mm glass test tubes, 5 mL and 20 mL serological pipets, micropipet ...


  • Performance-Based Measurement Systems

    Many of the Environmental Protection Agency's (EPA's) methods used to monitor air, water and soil for environmental contaminants prescribe step-by-step details on how the chemical analysis must be conducted and prohibit any deviations or variations. The EPA has recognized that monitoring equipment and technology have improved tremendously over the last few years; that environmental media do not ...


    By WSP | Parsons Brinckerhoff

  • Quantifying struvite formation in Calgary’s wastewater treatment system

    The paper presents a sampling and sample preparation protocol to evaluate struvite formation in the solids processing train of a wastewater treatment plant. The protocol was applied to the City of Calgary’s Bonnybrook and Fish Creek WWTP’s and the Shepard Sludge Lagoons. The soluble and particulate portions of magnesium, nitrogen and phosphorus (the chief components of struvite), as well as ...

  • Detection of PAH IN WATER using the ensys test system

    MATRIX: Water ANALYTES: PAH LIMIT OF DETECTION: 15 ppb MATERIALS: Ensys PAH Risc Soil Test Kit. Methanol (ACS Reagent Grade). Deionized water. Equipment: Ensys Field Accessory System. SAMPLE PREPARATION/ANALYSIS: Follow procedures are outlined in the Ensys PAH Risc Test Kit User’s ...


  • Analysis of PCB in water using the envirogard test system

    MATRIX: Water ANALYTE: PCB LIMIT OF DETECTION: Aroclor 1248: 1 ppm Aroclor 1260: 2 ppm Aroclor 1242: 2 ppm Aroclor 1254: 1.1 ppm BACKGROUND: This application describes a field screening method for determining PCB concentrations in water. A chemical reaction is induced that causes a color change ...


  • Tips to maintain your HPLC & UHPLC systems and columns

    Recently, Ade Kujore (Cecil Instruments), Tracie Brombos (GenTech Scientific) and I were asked by Angelo De Palma, a well-respected writer for Lab Manager magazine, to contribute to an article about maintaining and caring about your laboratory instruments. Here are my tips/best practices for column and HPLC/UHPC/UPLC system maintenance. Maintaining your ...


    By Waters Corporation

  • New laser-based dust emission monitoring system

    Abstract A new generation of continuous particulate matter concentration monitoring instruments is presented, covering a measuring range of 0 to 1000 mg/m3. The laser-based scattered light instrument gives an improved stability as well as excellent resolution in the low range. This enables high concentration measurement as well as especially low emission monitoring down to 0.01 mg/m3 with a ...


    By SIGRIST - PHOTOMETER AG

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