Food Quality Analysis Applications in Australasia

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    Increased Pigment Removal with Analysis of Pesticides in Oranges

    An application was developed to demonstrate increased pigment removal for the analysis of pesticides, using Supel™ QuE Z-Sep/C18 QuEChERS and an Ascentis® Express C18 HPLC Column. The improved cleanup can decrease column and instrument fouling, leading to extended LC column lifetime and reduced instrument downtime.

    By Merck KGaA, Darmstadt, Germany Office in AUSTRALASIA.

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    Analysis of Pesticides in Beef Kidney

    The suitability of the new cleanup sorbent, Supel QuE Z-Sep+, has been successfully demonstrated for cleanup of beef kidney matrix. It was found to effectively reduce background without significantly reducing recovery of lipophilic pesticides such as organochlorines and some pyrethroids. GC-MS full-scan data indicated Z-Sep+ was found to provide better cleanup in the form of reduced background than PSA/C18, and less interference in the GC-MS/SIM analysis of the target pesticides themselves.

    By Merck KGaA, Darmstadt, Germany Office in AUSTRALASIA.

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    Chromatography laboratory instrumentation for food & beverage

    Effective measures against food fraud, efficient and healthy food processing and the development of functional food and neutraceuticals are just few of many challenges in modern F&B production and analysis. BUCHI offers classical reference methods and near infrared spectroscopy (NIRS) for food analysis, but also visualization of production processes using spray drying and encapsulation.

    By BÜCHI Labortechnik AG Distributor in Noble Park North, AUSTRALIA.

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    Analysis of Methylimidazoles in Caramel Colored Carbonated Beverages

    Caramel colorings are used as additives in a broad range of food and beverage products to impart a desired color, but have no nutritional or preservative function. Recently, the potential hazard to humans of ammonia- and ammonia-sulfite-process caramel colorings was raised, because they contain the by-product 4-methylimidazole, which is a potential carcinogen.1 The methylimidazole compounds are difficult to analyze due to their polar nature and low molecular weight. Traditional reversed phase techniques are unsuccessful in retaining these small polar compounds. Therefore, most HPLC methods utilize ion-exchange resins for analysis. Another common method involves GC analysis after the analytes first undergo a derivatization step. The purpose of the work shown in this article was to develop a simple and fast analytical method to determine the levels of 2-methylimidazole and 4-methylimidazole in caramel colored carbonated beverages.

    By Merck KGaA, Darmstadt, Germany Office in AUSTRALASIA.

  • Increased Pigment Removal with Analysis of Pesticides in Oranges

    An application was developed to demonstrate increased pigment removal for the analysis of pesticides, using Supel™ QuE Z-Sep/C18 QuEChERS and an Ascentis® Express C18 HPLC Column. The improved cleanup can decrease column and instrument fouling, leading to extended LC column lifetime and reduced instrument downtime.

    By MilliporeSigma Office in Sydney, AUSTRALIA.

  • Analysis of Methylimidazoles in Caramel Colored Carbonated Beverages

    Caramel colorings are used as additives in a broad range of food and beverage products to impart a desired color, but have no nutritional or preservative function. Recently, the potential hazard to humans of ammonia- and ammonia-sulfite-process caramel colorings was raised, because they contain the by-product 4-methylimidazole, which is a potential carcinogen.1 The methylimidazole compounds are difficult to analyze due to their polar nature and low molecular weight. Traditional reversed phase techniques are unsuccessful in retaining these small polar compounds. Therefore, most HPLC methods utilize ion-exchange resins for analysis. Another common method involves GC analysis after the analytes first undergo a derivatization step. The purpose of the work shown in this article was to develop a simple and fast analytical method to determine the levels of 2-methylimidazole and 4-methylimidazole in caramel colored carbonated beverages.

    By MilliporeSigma Office in Sydney, AUSTRALIA.

  • Analysis of Pesticides in Beef Kidney

    The suitability of the new cleanup sorbent, Supel QuE Z-Sep+, has been successfully demonstrated for cleanup of beef kidney matrix. It was found to effectively reduce background without significantly reducing recovery of lipophilic pesticides such as organochlorines and some pyrethroids. GC-MS full-scan data indicated Z-Sep+ was found to provide better cleanup in the form of reduced background than PSA/C18, and less interference in the GC-MS/SIM analysis of the target pesticides themselves.

    By MilliporeSigma Office in Sydney, AUSTRALIA.

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