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Mass Spectrometry Applications

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    odor control for asphalt

    Control Asphalt Odors Naturally: The production of hot mix paving asphalt generates odors that can be strong, persistent, and a nuisance to employees and neighbors alike. Controlling and abating these odors can be a challenge.

    By OMI Industries (OMI) based in Long Grove, ILLINOIS (USA).

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    Analysis of VOC compounds in water by Purge & Trap or dynamic headspace

    Context & Challenges Volatile organic compounds (VOC) can be dissolved in water. Sometimes water is polluted and to study contamination of VOC in finished drinking water, VOC must be measured. Chromatotec® Solutions Chromatotec® has developed a specific system for the measurement of VOC in water: a Purge & Trap system, the airmoPURGE. The analyzer is coupled with a degasing system allowing the extraction of dissolved gases. The complete system is based on: - 502.2 method from US EPA – “Volatile organic compounds in water by purge and trap capillary column gas chromatography with photoionization and electrolytic conductivity detectors in series – Revision 2.1”. - 524.2 method from US EPA – “Measurement of purgeable organic compounds in water by capillary column gas chromatography/mass spectrometry – Revision 4.0”.

    By Chromatotec Group based in Val de Virvée, FRANCE.

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    Analytical instruments for mass spectrometry

    A variety of MS techniques – such as Quadrupole MS, Time-of-Flight (TOF) MS, Ion Mobility Spectroscopy (IMS), etc. have been developed in the past decades, providing new tools for materials analyses. Flow control for mass spectrometry (MS) requires high repeatability and small temperature- and pressure dependency. This is important to achieve a high resolution and instrument resolution. Depending on the size and electrical interface requirements, the Axetris MFC modules or MFC standalone types are the ideal choices for MS applications.

    By Axetris Ag based in Kaegiswil, SWITZERLAND.

  • Residual Gas Analysis

    Residual Gas Analysis is a general term for the analysis of gas and vapour species in vacuum chambers and vacuum processes. The Hiden RGA series quadrupole mass spectrometers provide for routine, fast, wide dynamic range residual gas analysis, measuring the partial pressures of the species that are critical to vacuum quality and process requirements. Applications include: vacuum chamber leak detection vacuum quality measurement and monitoring virtual leak detection outgassing studies bakeout cycle/vacuum pump down monitoring

    By Hiden Analytical Ltd. based in Warrington, UNITED KINGDOM.

  • End Point Detection

    Hiden Ion Milling Probe – End Point Detector The only dedicated end point determination tool for ion etch control and optimum process quality. End point Analysis. Target Impurity Determination. Quality Control / SPC. Residual Gas Analysis. Leak Detection The IMP is a differentially pumped, ruggedized secondary ion mass spectrometer for the analysis of secondary ions and neutrals from the ion mill process, featuring: High Sensitivity SIMS / MS with Pulse Ion Counting Detector. Triple filter Quadrupole, 300 amu mass range is standard. Differentially Pumped Manifold With Mounting Flange to Process Chamber. Ion Optics with Energy Analyser and integral ioniser. Penning Gauge and interlocks to provide over pressure protection. Data System with integration to the process tool. Stability (less than ±0.5% height variation over 24 h). MASsoft control via RS232, RS485 or Ethernet LAN. Programmable DDE, Parallel Digital I / O, RS232 Scripting Communication

    By Hiden Analytical Ltd. based in Warrington, UNITED KINGDOM.

  • MBE Desposition Rate Monitoring and Control

    XBS Triple Filter Quadrupoles configured for multiple source monitoring in MBE deposition applications. The custom configured ioniser provides for high stability, high senstivity monitoring of oxides and metals from both k-cell and e-gun sources. MBE monitoring and control. Molecular Beam Studies. Multiple beam source analysis. High Performance RGA. Desorption / Outgassing studies / Bakeout cycles. Chamber / Process gas Contaminants. Hiden XBS mass spectrometers for high precision scientific, process applications and MBE analysis, featuring: High Sensitivity, Enhanced detection from 100% to 5ppb, mass range to 510 amu. Enhanced long-term Stability (less than ±0.5% height variation over 24 h). Crossbeam ion source, beam acceptance through +/- 35° to transverse axis. Ion source control for soft ionisation and appearance potential mass spectrometry. Enhanced sensitivity for high mass transmission,

    By Hiden Analytical Ltd. based in Warrington, UNITED KINGDOM.

  • Mass Spectrometer for air consultancy

    Everyone has a responsibility to care for the environment to reduce the levels of pollution, including businesses that daily release emissions into the air and the ground. This is why we provide a full-service environmental testing service to help businesses identify problems and resolve them so they operate in the most environmentally-friendly method possible. We offer air emission testing, emissions monitoring services and stack emissions testing to businesses of all sizes.

    By Custom Stack Analysis, LLC. based in Alliance, OHIO (USA).

  • Thermal Analysis Mass Spectrometry

    Hiden offers optimized interface coupling to a range of thermal analysis systems including: TGA-MS and TGA/DTA-MS systems: Hiden Isochema IGA - intelligent gravimetric analyser, PerkinElmer-TA Instruments- Netzsch- Mettler Toledo- Seteram Calorimetry: Mass spectrometry for simultaneous evolved gas/calirometry analysis. Evolved gas analysis compliments the calorimetric data providing reaction kinetics data and speciation of reaction off gas. Solid Insertion Probe: An integrated solid insertion probe mass spectrometer system for in-situ TPD studies. Hiden Catlab: An integrated microreactor/mass spectrometer for catalyst characterisation.

    By Hiden Analytical Ltd. based in Warrington, UNITED KINGDOM.

  • Measurement solution for FTIR Vs. GC in gas analysis

    Comparison of Technologies

    A gas chromatograph (GC) has traditionally been the technology of choice for laboratory analysis of gas samples. GCs have been used for over 50 years in the qualification and quantification of complex mixtures of gases. The techniques and methodology required to run GCs are often a pre-requisite for any laboratory technician. Recent developments in Fourier Transform Infra-Red (FTIR) gas analysis has enabled this technology to start to replace GCs in the lab.

    By Protea Limited based in Middlewich, UNITED KINGDOM.

  • Catalysis

    Hiden's modular CATLAB offers a wide range of experimental tools for catalyst researchers, from rapid dynamic screening to fully automated precise investigations of active surface chemistry & optimisation of catalytic activity. The CATLAB performs analysis using temperature programmed methods such as TPR/TPO/TPD. Pulse chemisorption is also available with the CATLAB-PCS. The integrated QGA mass spectrometer system provides for quantification of the adsorbed/desorbed species. Physical analyses such as metal surface area, catalyst dispersion and surface acidity/basicity are provided. All CATLAB & mass spectrometer sampling wetted surfaces are designed to have the widest possible compatibility for use with aggressive species. Hiden Analytical’s HPR-20 QIC mass spectrometer is available for coupling to existing catalyst reactors with integral analysis software available for TPD/TPR/TPO quantification. A range of specialized connectors & couplings optimise integration with reactor vessel

    By Hiden Analytical Ltd. based in Warrington, UNITED KINGDOM.

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