Sample Preparation Applications

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  • Category: Monitoring & Testing ×

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Reduced Fat Interference with Analysis of Pesticides in Avocados

by Sigma-Aldrich Co., LLC     based in Bellefonte, PENNSYLVANIA (USA)

QuEChERS (Quick, Easy, Cheap, Effective, Rugged, Safe) is a very popular method for the extraction and cleanup of fruit and vegetable samples for pesticide residue analysis.2-4 The extraction step uses acetonitrile and a salting out effect (with MgSO4). Cleanup is then accomplished using dispersive SPE (dSPE) followed by a centrifuge step prior to analysis. This application shows the clean-up and analysis using Supel™ QuE Z-Sep+ QuEChERS and an SLB®-5ms GC column.

Application package Ash for analysing oxidic materials

by Fluxana GmbH Co. KG     based in Bedburg-Hau, GERMANY

This application package is a `ready to go` calibration kit for xrf instruments. Fusion technology is ideal for analysing oxidic materials like ashes. It performs with the highest precision possible in xrf sample preparation. Primarily power stations and their control laboratories have to check the ash from the burning process of black and brown coal. Two standard DIN and ASTM methods describe the testing in detail. FLUXANA is able to deliver both methods ready from the bench.

PTR-MS systems for medical sector

by Ionicon Analytik Ges.m.b.H.     based in Innsbruck, AUSTRIA

PTR-MS are powerful tools for non-invasive, real-time breath gas analysis with many applications, such as screening for disease markers, study of pharmacokinetics or metabolic processes.

PTR-MS systems for biological research

by Ionicon Analytik Ges.m.b.H.     based in Innsbruck, AUSTRIA

Real-time measurement of plant defense and leaf wounding reactions. Measurement of VOCs in dynamic biological systems with low detection limit and without sample preparation.

Application package raw materials

by Fluxana GmbH Co. KG     based in Bedburg-Hau, GERMANY

Fusion technology is ideal for analysing oxidic materials like minerals or raw materials. It performs with the highest precision possible in xrf sample preparation. However, many laboratories cannot specify exactly what material they have to analyse. Therefore FLUXANA has created a wide range oxidic application program to allow complete analysis of the unknown material. The concentration ranges and elements of interest can be adapted to customer needs. It contains all parts to perform a complete raw material (oxidic materials) calibration with 14 elements for cement, glass, ceramic and raw materials industry. FLUXANA application packages include always the sample preparation method. All packages are running in our application laboratory. You are always free to send your samples for testing free of charge. If you combine our application packages with our sample preparation machines FLUXANA garanties the analytical performance of the package like a contract.

Application package glass

by Fluxana GmbH Co. KG     based in Bedburg-Hau, GERMANY

This application package is a 'ready to go' calibration kit for xrf instruments. In the glass industry, raw materials have to be analysed together with the quality control samples from production. FLUXANA has created two basic programs Raw Materials (CS-0022) and Glass (CS-0016) for these two purposes, which can be individually adapted by the customer. FLUXANA application packages include always the sample preparation method. All packages are running in our application laboratory. You are always free to send your samples for testing free of charge. If you combine our application packages with our sample preparation machines FLUXANA garanties the analytical performance of the package like a contract.

XRF analysis for metals exploration & mining

by Niton UK Limited     based in Woodmancott, Winchester, UNITED KINGDOM

Niton instruments offer unprecedented performance for a variety of mining and metals exploration applications, all in the palm of your hand. Examples include: Geo-Chemical Exploration. Metal exploration and assessment. Survey & Ore-Body Assessment. Mine Mapping, Development & Grade Control. Mill Heads & Tailings. Smelter Operations. Environmental Monitoring. Mining & Mineral Assessment.

Improved Recovery of the Fungicide Carbendazim

by Sigma-Aldrich Co., LLC     based in Bellefonte, PENNSYLVANIA (USA)

Fungicide carbendazim can some times be used to combat mold on citrus fruits including oranges. Recently, low residue levels of the fungicide were reported to be present in the bulk orange juice import shipments to the USA. Because this compound can persist through processing steps and may be found in the final consumer product, many government agencies have established maximum residue limits (MRLs) to ensure the safety of their population. Presented here is a single method, involving fast and effective QuEChERS cleanup, suitable for various orange juice matrices. The choice of PSA/C18 sorbents reduced interferences, resulting in greater recoveries and less ion-suppression. Because the QuEChERS method is fast, it only adds a few minutes to the sample preparation procedure. Sample processing using QuEChERS with PSA/C18 allows analysts to accurately process various matrices in a single workflow, with very little additional sample preparation time.

Substitute fuel sampling system

by Erdwich Zerkleinerungssysteme GmbH     based in Kaufering, GERMANY

A critical eye for every sample! Analytical shredding systems for QA work are a fundamental preliminary component in the production of substitute fuels. With primary fuels and finite resources subject to continuous price increases, the significance of substitute fuels continues to rise unabated. For plant operators, this offers first-class potential and attractive prospects for the future. Businesses that buy in their substitute fuel from external suppliers are faced with two key analytical requirements before putting it to use: pollutant analysis and calorific analysis. To ensure the proper handling of these analyses, a sophisticated sampling system is required.

Application package cement

by Fluxana GmbH Co. KG     based in Bedburg-Hau, GERMANY

This application package is a `ready to go` calibration kit for xrf instruments. It contains all parts to perform a complete cement calibration: - Calibration set prepared from CRM as glass beads 40mm - Calibration work performed by FLUXANA expert 2 days on site - 2x drift monitors for xrf instrument - 2x control samples for validation each 10g powder for preparation on site - Flux FX-X100 FLUXANA application packages include always the sample preparation method. All packages are running in our application laboratory. You are always free to send your samples for testing free of charge. If you combine our application packages with our sample preparation machines FLUXANA garanties the analytical performance of the package like a contract.

XRF analysis for WEEE compliance & RoHS

by Niton UK Limited     based in Woodmancott, Winchester, UNITED KINGDOM

Niton instruments offer unprecedented performance for a variety of mining and metals exploration applications, all in the palm of your hand. Examples include: Geo-Chemical Exploration. Metal exploration and assessment. Survey & Ore-Body Assessment. Mine Mapping, Development & Grade Control. Mill Heads & Tailings. Smelter Operations. Environmental Monitoring. Mining & Mineral Assessment.

Filtration systems & solutions for biosciences and scientific industry

by Porvair Filtration Group     based in Fareham, UNITED KINGDOM

The scientific community and in particular for that of the life science industries such as the medical, pharmaceutical  and healthcare, have a growing need for superior technologies and products in filtration, separation, purification, aeration and liquid transfer. The range of BioVyon materials and applications are continuously expanding, driven by new market requirements and available to both OEM and end user customers. Applications include separation or filtration for healthcare, medical and pharmaceutical products, shut off valves for catheters, diagnostic wick and sample preparation devices.

Energy reduction and coagulation process control for wastewater treatment industry

by Pollution & Process Monitoring Ltd     based in Sevenoaks, UNITED KINGDOM

One of the biggest costs for water-water treatment is energy consumption; the cost of which is likely to escalate with increased demand. Ineffective process control may not only be costly but environmentally impacts though the inefficient use of an un-renewable resource. Furthermore, poor process control in one area may also impinge on neighbouring processes ultimately affecting effluent water quality.

Application package continous casting powder 'ready to go'

by Fluxana GmbH Co. KG     based in Bedburg-Hau, GERMANY

This application package is a 'ready to go' calibration kit for xrf instruments. Together with the company Stollberg, FLUXANA has developed a fused bead method for the product control of continuous casting (CC) powders. The general idea was a universal program which covers a wide product range and that is also able to control the used raw materials. The result was two different application packages each with a set of standards and a set of control samples. - Calibration set continuous casting powders prepared from CRM as glass beads - Calibration set raw materials prepared from CRM as glass beads - Calibration work performed by FLUXANA expert 2 days on site - 2x drift monitors for xrf instrument - 2x control samples for validation each 10g powder for preparation on site - Flux FX-X100 FLUXANA application packages include always the sample preparation method. All packages are running in our application laboratory. You are always free to send your samples for testing free of charge.

Improved Reproducibility and Reduced Sample Preparation Time for the HPLC Analysis of Aflatoxins in Raw Peanut Paste

by Sigma-Aldrich Co., LLC     based in Bellefonte, PENNSYLVANIA (USA)

The US FDA and international regulatory agencies have set contamination levels for aflatoxins in animal feedstuffs. Since Aspergillus may infect commodities pre-harvest, during storage or during processing, monitoring for aflatoxins in associated agricultural commodities at all stages of production is requisite. Field screening methods exist that are adequate to estimate contamination levels for aflatoxins. When additional confirmation or quantification is desired, chromatographic laboratory analysis is often necessary. Preparation of matrix samples prior to chromatographic analysis typically requires extraction and purification. Commonly, immunoaffinity columns (IAC), which employ a multi-step bind and elute mechanism to concentrate and purify aflatoxins, are used to purify matrix samples for subsequent analysis. Solid phase extraction (SPE), an alternate method which may use interference removal, can also be employed.

Analysis of Isocyanates Using the ASSET™ EZ4-NCO Dry Sampler

by Sigma-Aldrich Co., LLC     based in Bellefonte, PENNSYLVANIA (USA)

Isocyanates are used as a raw material to produce a number of products . Personal exposure can occur while the products made with isocyanates are being applied, or when the materials are removed by grinding or thermal degradation. Workers who are exposed to these compounds are at risk for respiratory disorders and asthma. The highly reactive nature of the isocyanate compounds and the low occupational exposure limits put high demands on both sampling and analytical techniques for monitoring of isocyanates in air. We investigated the performance of the LC-MS and LC-MS-MS methods in the analysis of isocyanates using the new ASSET™ EZ4-NCO Dry Sampler. We found that the analytical method can successfully reach the quantitation limit for most isocyanates of 5 ng/mL in the final sample when LC-MS-MS analysis was used and the quantitation limit of 10 ng/mL when LC-MS analysis was used. All 11 compounds were well-resolved chromatographically using a 15 cm Ascentis Express C18 column.

Application package for analysing slags and filter dusts

by Fluxana GmbH Co. KG     based in Bedburg-Hau, GERMANY

This application package is a `ready to go` calibration kit for xrf instruments. The analysis of slags and filter dusts in the metal industry delivers important information about the production process. FLUXANA has developed a fusion slag + filter dusts method which allows the direct analysis of most common slags and filter dusts. Elements of interest and calibrated concentration ranges can be selected individually by the customer.

Mixers, dryers, innovative solutions for environmental engineering

by AVA - Huep GmbH u. Co. KG     based in Herrsching, GERMANY

Applications in the field of environmental engineering have always counted among AVA’s core competencies. We are the innovation leader for numerous applications, and our machines are known for their heavy-duty designs and associated long service life.

Measurement solution for multi-stream combustion research

by Protea Limited     based in Middlewich, UNITED KINGDOM

Protea supplied a complete turn-key measuring system for multi-point sampling in a University combustion research laboratory. Utilising the latest in FTIR spectroscopy, atmosFIR, a complete cabinet system was supplied containing: atmosFIR FTIR Gas analyser, Sampling System Control Module (SSCM), Heated Stream Selection Module (HSSM), Temperature Control Module (TCM), 4 heated sample lines, 4 heated sample probes, Embedded PC controller.

Sample preparation and pumping systems for wastewater treatment industry

by Pollution & Process Monitoring Ltd     based in Sevenoaks, UNITED KINGDOM

A wide range of sample acquisition and filtration systems are available to prepare even the most difficult of samples for reliable on-line analyser measurement. The correct choice is often critical to prevent analyser blockage and optimise performance. Cross Flow Filtration The PPM cross flow filter, is a simple in-line device used to protect an analyser from ingress of solids, for applications where sample quality is generally good but occasionally suspended solids may be present. The stainless steel filter removes solids above 50 micron size.

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