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IDEXX BioAnalytics
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Small Molecule LC-MS/MS Services

Small Molecule LC-MS/MS Services

FromIDEXX BioAnalytics

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IDEXX BioAnalytics now provides high quality LC-MS/MS bioanalysis for small molecule compounds. In addition to standard protein precipitation, IDEXX BioAnalytics offers solid phase extraction and solid supported liquid extraction. We offer the same high-quality, flexible, and fast turnaround in our bioanalysis laboratory as we do for our current clinical and anatomic pathology services.

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solid phase extraction

triple quadrupole mass spectrometry

quadrupole mass spectrometry

solid-liquid extraction

mass spectrometry

refrigerated centrifuge

Sciex 5500+ Triple Quadrupole Mass Spectrometer

ESI source and APCI source

Shimadzu Nexera X2 HPLC
Integra Biosciences VIAFLO96 pipetting robot
Beckman Avanti JXN-26 refrigerated centrifuge
Mettler XPR36DR analytical balance
Biotage TurboVap96 evaporator
WinNonlin Phoenix software

Protein precipitation

Organic and acidic methods

Solid Phase Extraction
Solid Supported Liquid Extraction

Blood
Serum
Urine
Tissue homogenates

Method Feasability

Detecting the compound in the mass spectrometer

Compound infusion
Ionization parameter optimization

Eluting the retained compound from the UHPLC column

Column and mobile phase selection
Compound injection for retention time and peak shape assessment

Development and Pre-qualification

Optimizing the LC-MS/MS method
Accuracy

3 concentrations tested

Precision

3 concentrations tested
Quality control samples every 10 samples

Linearity

8 concentrations tested

Sensitivity

Limit of Detection