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Miprowa - Model Configuration II -Lab System
Never before have you been able to carry out tests so simply and so quickly which in the past were not manageable or hardly controllable using conventional equipment. Using the Miprowa® Lab laboratory reactor, you can measure temperatures at high sampling rates at various parts of the reaction process and also add additional materials to the two liquid reactants to, for example, carry out a quenching process. You would also like to vary the dwell time and other parameters such as pressure to gain a better knowledge of your process? This flexible construction may be put together from modules and the reaction quantities may be adjusted.
Miprowa® Lab may be used as an interface module together with micro equipment for process optimisation on a laboratory scale. Following this scale-up is carried out using an analogue channel design, that is to say with the same or similar dimensions of the rectangular flow channels, thus under the same process conditions as in the production scale. Miprowa® apparatus technology is distinguished by a high surface-to-volume ratio of the flow channels, continuous blending of the process flow and its flexibly modifiable apparatus design.
Automated micro-reactor system with flexible regulation and measurement of the reaction temperature. It is suited for continuous synthesis in liquid-liquid (both homogenous and also inhomogenous) and gaseous-liquid reaction mixtures in a temperature range of -20 to +200 °C. The system may be expanded as desired using additional functional modules of the MMRS.
Automated micro-reactor system with flexible regulation and measurement of the reaction temperature. It is suited for continuous synthesis in liquid-liquid (both homogenous and also inhomogenous) and gaseous-liquid reaction mixtures in a temperature range of -20 to +200 °C. The system may be expanded as desired using additional functional modules of the MMRS.
Specifications
Frame MRT-Rack™, anodised aluminium base plate for modules (A3 format)
Reactor 1 x Miprowa® Lab reactor with 30 ml interior volume spread across 8 rectangular channels with the dimensions 1.5 x 12 x 300 mm and static mixing elements, integrated temperature measurement (Pt100), process media connections via the MMRS (1/8", 1/16" Swagelok® or Valco), thermal media connections 12 mm Swagelok®, flange for 4/8 channel operation
Accessories: Dosing flange for up to 4 additional liquid supply lines or temperature controllers (1/16‘‘ Valco), reducing flanges for 2 or 6 channel operation; connection adapter for thermostats
Mixer Static micro-mixer: 1 x comb mixer (other micro-mixers available)
Modules 3 x inlet/outlet 1/8’‘ Valco, 2 x p sensor modules (100 bar), 1 x coaxial heat exchanger, many additional modules available
Heating/cooling system Heating/cooling thermostat(e. g. Lauda Proline RP845, Huber Ministat 230), working temperature range -45…+200 °C, heating power 2 kW, cooling power 0.38 kW at 0 °C
Accessories: insulated heating hoses, thermal oil
Dosing system 2 x SyrDos™ syringe pumps (for low-pressure applications)
2 x GearDos™ micro-tooth ring pumps (for higher pressures and higher flows)
Optional: Flow rate controller for micro-tooth ring pumps, pumps for additional dosing of further liquid flows, mass flow meter for the dosing of gases
Pressure range Max. 30 bar (dependent on the pump used), a pressure regulator may be an advantage when working with gases – obtainable as an MMRS module up to 25 bar working pressure
Sensors 2 x temperature sensors: Inlet and outlet of the Miprowa® reactor (optionally up to four additional ones in the dosing flange), 2 x pressure sensors: in front of the mixer
Automation LabBox® with the following equipment:
Interfaces: 8 Pt100 temperature measurement inputs, 8analogue inputs (current and voltage), 8 analogue outputs (current and voltage), 4 digital outputs (24 V AC), 4 digital outputs (44 V AC), 12 serial interfaces
Materials Base plate: Aluminium; parts in contact with media made of stainless steel or Hastelloy (standard, others available on request); seals in contact with media: FFKM otherwise FKM (others available on request)
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